By D. R. Bundle, G. Descotes, J. Gigg, R. Gigg, W. Klaffke, B. Meyer, J. Staněk, T. Suami, J. Thiem (auth.)
Contents: D.R. package, Ottawa, Ont., Canada: Synthesis of Oligosaccharides on the topic of Bacterial O-AntigensG. Descotes, Villeurbanne, France: Synthetic Saccharide PhotochemistryJ. Gigg, R. Gigg, London, united kingdom: Synthesis of GlycolipidsB. Meyer, Athens, GA, united states: Conformational elements of OligosaccharidesJ. Stanek, Jr., Prague, CSFR: Preparation ofSelectively Alkylated Saccharides as artificial IntermediatesT. Suami, Tokyo, Japan: Chemistry of Pseudo-SugarsJ. Thiem, W. Klaffke, Hamburg, FRG: Syntheses of Deoxy Oligosaccharides
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1 A c e t a t e s . . . . . . . . . . . 2 P i v a l o a t e s . . . . . . . . . . . 3 B e n z o a t e s . . . . . . . . . 5. I. 4 T r i f l u o r o m e t h a n e S u l f o n a t e s , T h i o c a r b a m a t e s a n d Xanthates . . . . . . . . . . . 2 P h o t o x i d a t i o n . . . . . . . . . . . . . 1 P h o t o x i d a t i o n o f P r o t e c t e d C a r b o h y d r a t e s . . . . . . 2 P h o t o d e g r a d a t i o n o f F r e e C a r b o h y d r a t e s .
2 P k o t o l y s i s o f O x o a l k y l g l y c o s i d e s . . . . . . . . . 60 60 60 61 62 62 5 Photoreduction and Photoxidation Reactions of Sugars . . . . . 1 P h o t o r e d u c t i o n . . . . . . . . . . . . . 1 P h o t o d e o x y g e n a t i o n . . . . . . . . . . 1. I. 1 A c e t a t e s . . . . . . . . . . . 2 P i v a l o a t e s . . . . . . . . . . . 3 B e n z o a t e s . . . . . . . . . 5. I.
5 Synthetic Brucella Oligosaccharides The structures of the classical A and M antigens of Brucella were recently shown to be hompolymers of 4,6-dideoxy-4-formamido-a-D-mannopyranose [102, 103]. The A antigen was an ~-l,2-1inked polymer, while the M antigen was also linear but was composed of a pentasaccharide repeating unit of four ~-1,2- and one ~-l,3-1inked residues. Synthesis of oligosaccharides with the A structure ranging from di- up to pentasaccharide have been completed. A common intermediate (108) was used to prepare either glycosyl donor 109 or glycosyl acceptor 110 molecules.